I-N-Benzyl-N-ethylaniline

1Lulwelo olunombala otyheli okhanyayo, olunyibilikayo kwi-ethanol nakwezinye izinyibilikisi zendalo, alunyibilikiyo emanzini.

2, Indlela yokuvelisa ifumaneka ngokuphendula i-ethyl aniline kunye ne-benzyl chloride. Kwiketile efakwe i-lead, yongeza i-ethyl aniline, yongeza i-benzyl chloride ngelixa upholisa, uvuselele iiyure ezili-10, uze uyigcine ishushu kwi-100°C iiyure ezili-12. Emva kokuhlamba ngesisombululo se-sodium hydroxide, imveliso egqityiweyo ifunyanwa ngokuhlanjululwa nge-vacuum. I-Diethylaniline ingasetyenziswa njengezinto eziluhlaza. Umlinganiselo we-molar we-diethylaniline kwi-benzyl chloride yi-2:1. Yongeza i-1% yesixa se-feed ye-diethylaniline ukuyixuba ne-iodine, uphendule kwi-150℃ iiyure ezingama-20, uze uxube nge-vacuum distill ukuze ufumane imveliso egqityiweyo.

3, Isetyenziswa njenge-intermediate dye. Isetyenziselwa ukwenza i-SF eluhlaza okotshani kunye nezinye iidayi eziluhlaza okwesibhakabhaka.

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