iindaba

N-Benzyl-N-ethylaniline

1Lulwelo olunamafutha omthubi olukhanyayo, olunyibilikayo kwi-ethanol nakwezinye izinyibilikisi zendalo, ezinganyibilikiyo emanzini.

2, Indlela yokuvelisa ifumaneka ngokusabela ethyl aniline kunye ne-benzyl chloride. Kwi-kettle ehamba phambili, yongeza i-ethyl aniline, yongeza i-benzyl chloride ngelixa upholisa, ugxobhoze iiyure ezili-10, uze uhlale ushushu kwi-100 ° C kwiiyure ze-12. Emva kokuhlamba ngesisombululo se-sodium hydroxide, imveliso egqityiweyo ifunyenwe nge-vacuum distillation. I-Diethylaniline nayo ingasetyenziswa njengento ekrwada. Umlinganiselo we-molar we-diethylaniline kwi-benzyl chloride yi-2:1. Yongeza i-1% yomthamo wesondlo se-diethylaniline ukuze udibanise ne-iodine, uphendule kwi-150℃ nge-20h, kunye ne-vacuum distill ukufumana imveliso egqityiweyo.

3,Isetyenziswa njengedayi ephakathi. Isetyenziselwa ukwenza i-SF ekhanyayo eluhlaza kunye nezinye iidayi eziluhlaza.

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Ixesha lokuposa: Jul-26-2024